Course Contents
1- Molecular spectrophotmetry
Determination of iron(II) using 1,10-phenonthroline method, Determination of Iron(III) using thiocyanate method. Determination of chromium by diphenylcarbazie method
Determinatio nof Fe, Pb, Cd, Zn and Cu in soil samples by AAS technique. Simple acid base titrations using potentiometer
Determination of "F" in water by using ion selective electrodes, Preparation of standard calibration graphs of Pb, Cd, Zn and Fe by AAS. Determination of Ni by DMG method spectrophotometrically. Determination of mixtures of complexes of iron with thiocyanide and 1,10-phenonthroline
Determination of wavelength-max of Cr complex with diphenyl carbazide
infrared determination of a mixture of Xylene. spectrophotometric determination of lead or leaves using solvent extration
2- Conductometry
Determination of HCl conductometrically by using strong base NaOH, Determine the amount of base NH4OH conductometrically by using strong acid
Determine the amount of base NH4OH conductometrically by using weak acid CH3COOH, Determine the amount of NaOH conductometrically by using weak acid CH3COOH
3-Potentiometry
Determine the amount of HCl using strong base (NaOH) potentiometrically, Determine the amount of HCl using weak base (NH4OH) potentiometrically, Determine the amount of CH3COOH using strong base (NaOH) potentiometrically,
Determine the amount of HCl & CH3COOH using strong base (NaOH)
Course Synopsis
This course is based on the hands-on training of the students studying Analyitcal Chemistry for various experiments. This will include the problem solving and calculation-based learning towards analytical chemistry experiments.
Course Learning Outcomes
The student will learn
how to operate the spectrophotometer
how to perform experiments using spectrophotometers
how to obtain data and treat it in a scientific way
how to perform titrations using advanced methods including conductometer and potentiometer
They will also learn how to perform analysis using real samples.
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Book Title : Vogel's Quantitative Chemical Analysis
Author : Jeffery, Bessett, Mendham, Denny
Edition : 5
Publisher : Longman Scientific and Technical, USA
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